Different algorithms have been proposed to detect semantic shifts (changes in a word meaning over time) in a diachronic corpus. Yet, and somehow surprisingly, no reference corpus has been designed so far to evaluate them, leaving researchers to fallback to troublesome evaluation strategies. In this work, we introduce a methodology for the construction of a reference dataset for the evaluation of semantic shift detection, that is, a list of words where we know for sure whether they present a word meaning change over a period of interest. We leverage a state-of-the-art word-sense disambiguation model to associate a date of first appearance to all the senses of a word. Significant changes in sense distributions as well as clear stability are detected and the resulting words are inspected by experts using a dedicated interface before populating a reference dataset. As a proof of concept, we apply this methodology to a corpus of newspapers from Quebec covering the whole 20th century. We manually verified a subset of candidates, leading to QC-FR-Diac-V1.0, a corpus of 151 words allowing one to evaluate the identification of semantic shifts in French between 1910 and 1990.